Anyone perform a dual stage or mixed extraction?

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I was wondering if anyone has tried a dual stage extraction or mixed a cold maceration with a warm extraction? I am asking because from all my reading cold and warm extractions each seem to pull different flavors from the tobacco. Mixing NET extracted both ways or actually doing a dual extraction on the same batch of tobacco would seem like it would give the complete flavor palette.

Currently deployed so can't test this yet but I was thinking of trying this method when I get home in a few months.

1. Mix tobacco with a "priming" batch of PG (say 1oz tobacco and 30ml PG) in a heavy duty ziploc bag. You only want just enough that the tobacco will soak it all up so someone help if I got the ratio wrong. Squeeze the air out and throw it in the freezer overnight. Let it thaw out the next day, then freeze again. Thaw and freeze a third time. (This is to help with the flavor extraction).

2. Place tobacco onto square of cheese cloth and tie off. Place in Hermes Jar and add ~300% PG (example would be 90ml). Seal jar and store for about a month, gently swirling every few days.

3. Pour extract through metal mesh coffee filter into half pint Mason Jar and seal. Set jar aside for later.

4. Add ~10% PGA (3ml in example) and ~200% PG (60ml in example) to Hermes Jar with tobacco, seal jar and swirl gently to blend.

5. Place Hermes Jar in pressure cooker and simmer at ~180f for 8 hours, then turn off and open cooker. Let cool for 16 hours. Repeat the cycle, gently swirling the jar and topping off water between cycles.

6. Pour warm extract through mesh coffee filter into half pint Mason Jar with cold extract. Wrap cheese cloth in a coffee filter and gently squeeze over mesh filter to finish extract.

7. Pressure filter through a coffee filter (going to use an Aeropress for this step).

8. Hybid pressure/vacuum filter through a 5-micron absolute filter, then through a 2-micron absolute filter.


Has anyone here considered using aquarium air and water pumps? I have several aquariums and a bunch of experience with them, so they popped into my head right away. Quiet, fairly cheap, and designed to run on 110v without having to rig anything. There are also inline water blocks to keep from accidently sucking up any of your extract into your air pump that is generating your vacuum.

A hybrid filter would generate a vacuum under the filter and pressure above the filter. You can do this with a single pump if the intake is pulling air out from below the filter and the output is going in above the filter. Would generate a smooth flow with lower total pressure throughout. :D

So, what do all of the people who have been producing NETs think? Any tweaks, changes, or improvements recommended?
 

Str8vision

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I was wondering if anyone has tried a dual stage extraction or mixed a cold maceration with a warm extraction?...............................
............................So, what do all of the people who have been producing NETs think? Any tweaks, changes, or improvements recommended?

I retired from the Army Corps of Engineers, many of my colleagues served time in that locale, a few still do. Many interesting stories indeed. Welcome to the extraction forum.

I tried blending hot and cold PG macerations but for my taste the results were no better than just leaving them separate. There are no steadfast rules when it comes to extracting tobacco, the trick is to find what method works best for your individual taste preference. I currently use a sequential PGA (cold) followed by PG (hot), mix the two together and evaporate off most of the PGA. You ask for feedback on your ideas/planed method, I can offer a few observations and comments;

Dampening tobacco with PG and subjecting it to freeze/thaw cycles likely wont yield the results you are after. PG does not freeze or expand at the temperatures you will be able to achieve, the viscosity changes (it thickens a little), and that's about it. If anything, freezing a PG/tobacco mix will impede/slow saturation of the tobacco. When it comes to freezing, cellular disruption in organic matter can only be obtained when some degree of water is present as water expands when turned to a solid.

Enclosing the tobacco in cheese cloth (or other material), hinders the circulation/exchange of solvent around the tobacco obstructing flavor extraction. The only remedy to this would be to move the solvent under pressure through the encased tobacco via a circulation pump. I really don't think swirling alone could do it but you never know till you've tried.

Heating PG/PGA macerated tobacco to 180F for prolonged periods turns the tobacco into mush, been there done that losing several test batches along the way. I no longer use PGA (at any percentage), when heat is used for the extraction. PGA becomes "very aggressive" at elevated temperatures leeching out undesirable elements contained in the tobacco. Even when using straight PG I no longer heat above 150F and prefer 140F but I do 110 hour+ extractions. I don't do high heat/short duration extractions but others here have and perhaps they can help you along those lines.

I haven't tried using an aquarium pump to circulate extractions through a filter. When using absolute rated filters the flow rate can be quite slow (even under vacuum), as they provide considerable resistance to the flow of fluids especially those with the viscosity of PG or thicker. I do use a small DC vacuum pump when filtering below 2 microns and it works great. Above 2 microns I just let gravity and time do the work if I'm not in a hurry. No matter how you do it, filtering is much faster/easier when the temperature of the solvent is maintained above 70F, the warmer the better. If you do experiment with a recirculating pump let us know how it works. I have considered using a small recirculating pump to move solvent slowly/gently through the tobacco during the extraction process, taking the place of periodic swirling. I believe doing so might speed the flavor extraction process but it might also break the tobacco down rendering more plant matter in the solvent. Never know till you try.

Good luck with your efforts and be sure and post observations/results.
 
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