Full PDF Version will be on our Websites "About the Fluid page"
Scientific Analysis Laboratories
CERTIFICATE OF ANALYSIS
Report Number: 1610083
Date of Report:
Client: Pillbox 38 (UK) Ltd
Suite 3a Brookmill Complex
Branch Road
Lower Darwen
Lancashire
BB3 0PR
Client Contact: Mr Jason Cropper
Client Job Reference: Totally Wicked ESmoking
Liquid
Date Job Received at SAL: 01April2009
Date Analysis Started: 07April2009
The results reported relate to samples received at the laboratory
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation
This report should not be reproduced except in full without the written approval of the laboratory
Tests covered by this certificate were conducted in accordance with SAL SOPs
Key to symbols used in this report:
W: Analysis was performed at another SAL laboratory
S: Analysis was subcontracted
N: Analysis is not UKAS accredited
U: Analysis is UKAS accredited
Report written by: C. Rodger
Laboratory Manager
Report checked R. Hare
and authorised by: Laboratory Manager (Air Division)
14th July 2009
Produced by: Scientific Analysis Laboratories Ltd. Hadfield House, Hadfield Street, Manchester. M16 9FE
Page 2 of 4
Analysis of the Content of Totally Wicked ESmoking
Liquid supplied by Pill Box 38 (UK) Ltd
A sample of Totally Wicked ESmoking
Liquid was supplied to Scientific Analysis Laboratories Limited, to
determine the percentage level of nicotine it contained and other compounds present. The sample was analysed
by Gas Chromatography Mass Spectrometry.
The sample supplied was a 30ml bottle of 36mg Super High eliquid.
The Nicotine level was found to be : 1.8% (w/w)
The following pages of this report, give a more detailed breakdown of the analysis and details of other
compounds found
Note: On the following pages the term LOD means Limit of Detection, this is the lowest amount of a sample that can be
detected using the technique GC/MS (Gas Chromatography Mass
Spectrometry).
Produced by: Scientific Analysis Laboratories Ltd. Hadfield House, Hadfield Street, Manchester, M16 9FE
Page 3 of 4
Supplement to Report Number: 1610083
Client Job Reference:
SAL Ref: 161008 001
Client Ref: Pillbox 38 (UK) Ltd
Type: Oil
Ingredients Method Units LOD Symbol
Tobacco essencial oil n/a % n/a N <5%
Tobacco leaf oil n/a % n/a N <5%
Nicotine (from tobacco leaf) n/a % n/a N <3%
2,3,5Trimethylpyrazine
n/a % n/a N <1%
2,3,5,6Tetramethylpyrazine
n/a % n/a N <1%
2,5Dimethylpyrazine
n/a % n/a N <1%
2Acetypyrazine
n/a % n/a N <1%
2Methyl
butyric acid n/a % n/a N <1%
Terp ineol n/a % n/a N <1%
Ethyl maltol n/a % n/a N <1%
Guaiacol n/a % n/a N <1%
Acetyl pyridine n/a % n/a N <2%
Octalactone (gamma) n/a % n/a N <1%
Pure water n/a % n/a N <10%
Propylene Glycol n/a % n/a N >65%
Glycerol n/a % n/a N <20%
Totally Wicked ESmoking
Liquid
Produced by: Scientific Analysis Laboratories Ltd. Hadfield House, Hadfield Street, Manchester, M16 9FE
Page 4 of 4
Supplement to Report Number: 1610083
Client Job Reference:
SAL Ref: 161008 001
Client Ref: Pillbox 38 (UK) Ltd
Type: Oil
Semi Volatile Organic Compounds Screen Method Units LOD Symbol
Nicotine GC/MS % 0.001 N 1.8
Triethylene Glycol* GC/MS % 0.001 N 0.055
Tetraethylene Glycol* GC/MS % 0.001 N 0.078
Pentaethylene Glycol* GC/MS % 0.001 N 0.040
This sample was analysed using an Agilent 6890 GC5973
MSD operated in scanning mode from 35450
m/z.
Compounds detected were subjected to a library search with results confirmed by the operator.
*Results are semi quantitative
Scientific Analysis Laboratories
CERTIFICATE OF ANALYSIS
Report Number: 1610083
Date of Report:
Client: Pillbox 38 (UK) Ltd
Suite 3a Brookmill Complex
Branch Road
Lower Darwen
Lancashire
BB3 0PR
Client Contact: Mr Jason Cropper
Client Job Reference: Totally Wicked ESmoking
Liquid
Date Job Received at SAL: 01April2009
Date Analysis Started: 07April2009
The results reported relate to samples received at the laboratory
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation
This report should not be reproduced except in full without the written approval of the laboratory
Tests covered by this certificate were conducted in accordance with SAL SOPs
Key to symbols used in this report:
W: Analysis was performed at another SAL laboratory
S: Analysis was subcontracted
N: Analysis is not UKAS accredited
U: Analysis is UKAS accredited
Report written by: C. Rodger
Laboratory Manager
Report checked R. Hare
and authorised by: Laboratory Manager (Air Division)
14th July 2009
Produced by: Scientific Analysis Laboratories Ltd. Hadfield House, Hadfield Street, Manchester. M16 9FE
Page 2 of 4
Analysis of the Content of Totally Wicked ESmoking
Liquid supplied by Pill Box 38 (UK) Ltd
A sample of Totally Wicked ESmoking
Liquid was supplied to Scientific Analysis Laboratories Limited, to
determine the percentage level of nicotine it contained and other compounds present. The sample was analysed
by Gas Chromatography Mass Spectrometry.
The sample supplied was a 30ml bottle of 36mg Super High eliquid.
The Nicotine level was found to be : 1.8% (w/w)
The following pages of this report, give a more detailed breakdown of the analysis and details of other
compounds found
Note: On the following pages the term LOD means Limit of Detection, this is the lowest amount of a sample that can be
detected using the technique GC/MS (Gas Chromatography Mass
Spectrometry).
Produced by: Scientific Analysis Laboratories Ltd. Hadfield House, Hadfield Street, Manchester, M16 9FE
Page 3 of 4
Supplement to Report Number: 1610083
Client Job Reference:
SAL Ref: 161008 001
Client Ref: Pillbox 38 (UK) Ltd
Type: Oil
Ingredients Method Units LOD Symbol
Tobacco essencial oil n/a % n/a N <5%
Tobacco leaf oil n/a % n/a N <5%
Nicotine (from tobacco leaf) n/a % n/a N <3%
2,3,5Trimethylpyrazine
n/a % n/a N <1%
2,3,5,6Tetramethylpyrazine
n/a % n/a N <1%
2,5Dimethylpyrazine
n/a % n/a N <1%
2Acetypyrazine
n/a % n/a N <1%
2Methyl
butyric acid n/a % n/a N <1%
Terp ineol n/a % n/a N <1%
Ethyl maltol n/a % n/a N <1%
Guaiacol n/a % n/a N <1%
Acetyl pyridine n/a % n/a N <2%
Octalactone (gamma) n/a % n/a N <1%
Pure water n/a % n/a N <10%
Propylene Glycol n/a % n/a N >65%
Glycerol n/a % n/a N <20%
Totally Wicked ESmoking
Liquid
Produced by: Scientific Analysis Laboratories Ltd. Hadfield House, Hadfield Street, Manchester, M16 9FE
Page 4 of 4
Supplement to Report Number: 1610083
Client Job Reference:
SAL Ref: 161008 001
Client Ref: Pillbox 38 (UK) Ltd
Type: Oil
Semi Volatile Organic Compounds Screen Method Units LOD Symbol
Nicotine GC/MS % 0.001 N 1.8
Triethylene Glycol* GC/MS % 0.001 N 0.055
Tetraethylene Glycol* GC/MS % 0.001 N 0.078
Pentaethylene Glycol* GC/MS % 0.001 N 0.040
This sample was analysed using an Agilent 6890 GC5973
MSD operated in scanning mode from 35450
m/z.
Compounds detected were subjected to a library search with results confirmed by the operator.
*Results are semi quantitative